氟化物与石英光纤间的熔接参数优化与性能测试

Optimization of splicing parameters and performance testing between fluoride and silica fibers

  • 摘要: 基于偏置热熔接法,系统分析了熔接过程中各参数对熔接效果的影响及作用机理,探索出一种高效且广泛适用的氟化物光纤与石英光纤之间的熔接工艺。在探索单模氟铟光纤与单模石英光纤之间最佳熔接的过程中,提出了基于热膨胀性能差异形成可靠熔接点的大包小结构,并针对加热时间、加载功率、偏置、推进量等对熔接结果影响较大的参数做定量分析,通过对比熔点在不同参数下的损耗与机械强度以及熔接效果图,得到了普适性的最佳加热时间以及熔点损耗及强度随功率、偏置、推进量的变化趋势。实现了单模氟铟光纤与单模石英光纤之间的高质量熔接,熔点损耗低至0.04 dB,机械强度高于150 MPa,用高功率中红外超连续(MIR-SC)源重复泵入石英光纤9.6 W,熔点温度始终低于40 ℃,证明熔点具备高损伤阈值与长期稳定性。通过所述的熔接工艺,快速实现了石英光纤与氟碲酸盐光纤、ZBLAN光纤之间的高质量熔接,熔点损耗均小于0.1 dB,验证了该工艺的广泛适用性。此熔接工艺为中红外高功率全光纤激光器的进一步发展奠定了坚实的基础,具有很强的实用价值。

     

    Abstract:
    Objective This study systematically analyzed the impact and mechanism of various parameters on the efficacy of fusion splicing and explored an efficient and widely applicable fusion splicing technology between fluoride fiber and silica fiber. By investigating the optimal splicing parameters between single-mode indium fluoride fiber and single-mode silica fiber, we introduced the large-package-small structure concept, which establishes a reliable fusion point based on the significant difference in thermal expansion performance. We quantitatively analyzed key splicing parameters such as heating time, power, offset, and hot push that greatly influence the splicing outcome. The relationships between heating time, splicing loss, tensile strength, power, offset, and hot push were established by comparing splicing outcomes under different parameters. This research successfully achieved high-quality fusion splicing between single-mode indium fluoride fiber and single-mode silica fiber, with a minimal splicing loss of 0.04 dB and a tensile strength exceeding 150 MPa. Furthermore, the fusion point's temperature remained below 40 ℃ when subjected to a 9.6 W pumping test with a mid-infrared supercontinuum source, demonstrating high damage threshold and long-term stability. Additionally, high-quality fusion splicing was accomplished between silica fiber, fluorotellurite fiber, and ZBLAN fiber, resulting in a splicing loss of less than 0.1 dB, thereby confirming the broad applicability of the technology. These findings serve as a solid foundation for the advancement of mid-infrared high-power all-fiber lasers.
    Methods The study analyzed the principle of the offset thermal splicing method and identified its inability to yield a stable splicing point. As an alternative, the large-package-small structure concept was proposed, leveraging the thermal expansion coefficient difference between fluoride fiber and silica fiber to create a stable splicing point. Building upon this concept, the study elucidated the action mechanism of each parameter in the fusion splicing process and determined the splicing loss and tensile strength trends with each parameter through quantitative analysis of heating time, power, offset, and hot push. A laboratory fusion splicing process was developed based on this technology, and its reliability was validated through fusion splicing experiments involving silica fiber with ZBLAN and silica fiber with fluorotellurite fiber.
    Results and Discussions Under the optimal fusion splicing parameters for single-mode indium fluoride fiber and single-mode silica fiber, a splicing loss as low as 0.04 dB and a tensile strength exceeding 150 MPa were achieved at lower power levels. Moreover, the temperature of the fusion-splicing point remained below 40 ℃ during testing with a 9.6 W mid-infrared supercontinuum source, indicating high damage threshold and long-term stability. Fusion splicing between silica fiber and fluorotellurite fiber, as well as silica fiber and ZBLAN fiber, resulted in splicing losses of less than 0.1 dB and satisfactory tensile strength, affirming the technology's reliability.
    Conclusions  This study highlights the effectiveness of the offset thermal fusion splicing method through the fusion of single-mode indium fluoride fiber and single-mode silica fiber. By establishing a mature laboratory fusion splicing technology, the research achieved a high-quality fusion-splicing point with ultra-low loss, high tensile strength, high damage threshold, and long-term stability. The technology's reliability was confirmed through fusion splicing experiments involving silica fiber with fluorotellurite fiber and silica fiber with ZBLAN fiber, underscoring its significant potential in the realm of high-power all-fiber mid-infrared fiber lasers.

     

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