Volume 48 Issue S2
Oct.  2019
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Di Zhigang, Wang Biao, Yang Jiantan, Jia Chunrong, Zhang Jingxuan, Yao Jianquan, Lu Ying. Trace detection of pyridine based on HCPCF SERS sensor[J]. Infrared and Laser Engineering, 2019, 48(S2): 38-46. doi: 10.3788/IRLA201948.S213004
Citation: Di Zhigang, Wang Biao, Yang Jiantan, Jia Chunrong, Zhang Jingxuan, Yao Jianquan, Lu Ying. Trace detection of pyridine based on HCPCF SERS sensor[J]. Infrared and Laser Engineering, 2019, 48(S2): 38-46. doi: 10.3788/IRLA201948.S213004

Trace detection of pyridine based on HCPCF SERS sensor

doi: 10.3788/IRLA201948.S213004
  • Received Date: 2019-04-01
  • Rev Recd Date: 2019-05-14
  • Publish Date: 2019-09-30
  • Food is the paramount necessity of the people, safety is the first concern for the food, under the background of widespread application of various pesticides and food additives, illegal food additives have a serious impact on the food safety situation, and the qualitative detection of trace amounts of illegal food additives is of great significance. In order to achieve qualitative detection of pyridine, a sensing system based on HCPCF (Hollow Core Photonic Crystal Fiber) SERS was proposed. Silver nanoparticles were used to make SERS substrate, and SERS signal devices were designed to collect SERS in the same direction. By means of cone pulling on HCPCF to achieve selective filling, the detection scheme of collecting output signals by spectrometer was implemented. After the liquid pyridine sample with the concentration of 0.004 975% was detected, the obvious SERS characteristic spectrum could be observed. The experimental results show that the sensing system can achieve qualitative trace detection of pyridine in the liquid sample.
  • [1] Wang Hongli, Liu Suli, Zhao Mei, et al. Research progress on the harm of illegal addition of industrial dyes in food[J]. Journal of Food Safety and Quality, 2019, 10(1):1-7.
    [2] The Ministry of Health of the P.R. China, Standardization Administration of the P.R. China. GB5749-2006. Standards for drinking water quality, the national standard of the P.R. China[S]. Beijing:China Standard Press, 2007:2-4. (in Chinese)
    [3] National Environmental Protection Agency, The State Bureau of Technical Supervision. GB 15618-1993. Water quality-determination of pyridine-gas chromatography[S]. Beijing:China Standards Press, 1993.
    [4] Geng Y, Xu Y, Tan X, et al. A simplified hollow-core photonic crystal fiber SERS probe with a fully filled photoreduction pilver nanoprism[J]. Sensors, 2018, 18(6):1726.
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    [7] Cheng Ziqiang, Shi Haiquan, Yu Ping, et al. Surface-enhanced Raman scattering efect of silver nanoparticles array[J]. Acta Physica Sinica, 2018, 67(19):197302. (in Chinese)
    [8] Yao Jianquan, Di Zhigang, Jia Chunrong, et al. Photonic crystal fiber SERS sensors[J]. Infrared and Laser Engineering, 2011, 40(1):96-106. (in Chinese)
    [9] Di Zhigang, Jia Chunrong, Yao Jianquan, et al. Optimization on HCPCF SERS sensor based on silver nanoparticles[J]. Infrared and Laser Engineering, 2015, 44(4):1317-1322. (in Chinese)
    [10] Cordeiro C M B, de Matos C J S, dos Santos E M, et al. Towards practicalliquid and gas sensing with photonic crystal fibers:side access to the fiber microstructure and single-mode liquid-core fiber[J]. Measurement Science and Technology, 2007, 18(10):3075-3081.
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    [14] Creighton J A, Blatchford C G, Albrecht M G, et al. Plasma resonance enhancement of Raman scattering by pyridine adsorbed on silver or gold sol particles of size comparable to the excitation wavelength[J]. J Chem Soc, 1979, 75:795-798.
    [15] Liu R, Zi X, Kang Y, et al. Surface-enhanced Raman scattering study of human serum on PVA Ag nanofilm prepared by using electrostatic selfassembly[J]. Journal of Raman Spectroscopy, 2015, 42(2):137-144.
    [16] Di Zhigang, Yao Jianquan, Zhang Peipei, et al. Simulation and optimization of SERS effect in nano Ag substrates[J]. Laser Infared, 2011, 41(8):850-855. (in Chinese)
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Trace detection of pyridine based on HCPCF SERS sensor

doi: 10.3788/IRLA201948.S213004
  • 1. College of Electrical Engineering,North China University of Science and Technology,Tangshan 063210,China;
  • 2. Key Lab of Opto-electronics Information Science and Technology,Ministry of Education,College of Precision Instrument and Optoelectronics Engineering,Tianjin University,Tianjin 300072,China

Abstract: Food is the paramount necessity of the people, safety is the first concern for the food, under the background of widespread application of various pesticides and food additives, illegal food additives have a serious impact on the food safety situation, and the qualitative detection of trace amounts of illegal food additives is of great significance. In order to achieve qualitative detection of pyridine, a sensing system based on HCPCF (Hollow Core Photonic Crystal Fiber) SERS was proposed. Silver nanoparticles were used to make SERS substrate, and SERS signal devices were designed to collect SERS in the same direction. By means of cone pulling on HCPCF to achieve selective filling, the detection scheme of collecting output signals by spectrometer was implemented. After the liquid pyridine sample with the concentration of 0.004 975% was detected, the obvious SERS characteristic spectrum could be observed. The experimental results show that the sensing system can achieve qualitative trace detection of pyridine in the liquid sample.

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